Electron Backscatter Diffraction (EBSD) Analysis

Parameter Specification
Technique Electron Backscatter Diffraction (EBSD)
Operating Platform FESEM-based EBSD system
Spatial Resolution ~20–50 nm (material and setup dependent)
Angular Resolution ~0.5°
Mapping Modes Orientation mapping, phase mapping
Grain Analysis Grain size, grain boundary character
Texture Analysis Pole figures, inverse pole figures
Phase Discrimination Yes (crystalline phases)
Sample Type Metals, alloys, ceramics, crystalline materials
Sample Surface Highly polished, strain-free surface required
Sample Preparation Precision grinding, polishing, vibratory polishing
Information Obtained Grain orientation, texture, phase distribution
Typical Use Cases Metallurgy, ceramics, thin films, failure analysis
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Description

Advanced Electron Backscatter Diffraction service for crystallographic orientation, grain structure, and phase mapping of materials at the microscale. EBSD enables quantitative correlation between microstructure, texture, and material performance, particularly in polycrystalline and engineered materials.

Key Applications

  • Grain size and grain boundary analysis

  • Crystallographic orientation and texture mapping

  • Phase identification and phase distribution

  • Deformation, recrystallization, and failure analysis

  • Process optimization and quality assessment

Specifications

Parameter Specification
Technique Electron Backscatter Diffraction (EBSD)
Operating Platform FESEM-based EBSD system
Spatial Resolution ~20–50 nm (material and setup dependent)
Angular Resolution ~0.5°
Mapping Modes Orientation mapping, phase mapping
Grain Analysis Grain size, grain boundary character
Texture Analysis Pole figures, inverse pole figures
Phase Discrimination Yes (crystalline phases)
Sample Type Metals, alloys, ceramics, crystalline materials
Sample Surface Highly polished, strain-free surface required
Sample Preparation Precision grinding, polishing, vibratory polishing
Information Obtained Grain orientation, texture, phase distribution
Typical Use Cases Metallurgy, ceramics, thin films, failure analysis

 

Sample Preparation Support

  • EBSD-specific mechanical and vibratory polishing

  • Damage and deformation layer removal

  • Conductive coating guidance (if required)

  • Surface quality validation prior to mapping

  • (EBSD data quality is critically dependent on surface preparation and strain-free conditions.)

Deliverables

  • Orientation maps and phase maps

  • Grain size and grain boundary statistics

  • Texture plots (pole figures, IPFs)

  • Indexed EBSD datasets

  • Expert interpretation linked to processing and performance

Who Should Use This Service

  • Metallurgy and materials engineering teams

  • Ceramic and crystalline material researchers

  • Failure analysis and deformation studies

  • Industrial process development groups

Important Note

EBSD is sensitive to surface damage and crystallinity.
Amorphous materials or poorly prepared surfaces may not yield indexable patterns and may require complementary techniques such as TEM or XRD.

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